The laboratory unit is designed to study the catalytic and thermal processes of processing heavy oil feedstock.
The installation allows you to explore the processes:
- Hydrocracking;
- Thermal cracking;
- Gasification of aqueous dispersions of coal, biomass, heavy oil residues.
The developed high-pressure liquid pump operates at temperatures up to 200°C, which makes it possible to feed high-viscosity components (fuel oil, tar, paraffin, ceresin, etc.) into the reactor.
The laboratory unit is manufactured in accordance with the technical requirements of the customer to operate in a wide range of process parameters. The modular configuration of the unit allows it to be changed or upgraded at any time to meet new challenges.
Main advantages:
- The possibility of developing and supplying the reactor according to the requirements of the customer;
- Wide range of liquid/solid supply accessories;
- Visual process control;
- System of control and regulation of technological parameters;
- Convenience of loading and unloading of feedstock and reaction products;
- The possibility of conducting long-term tests in continuous mode;
- The possibility of modernizing the design for new purposes;
- Control and precise reproduction.
Completeness (the final delivery set depends on the terms of reference):
- Unit for preparation of gas-phase raw materials;
- Block for preparation of carbonaceous raw materials;
- Block of supply of carbonaceous raw materials;
- Reactor block;
- Separation, cleaning and drying unit;
- Sampling unit;
- Unit for measuring the volume of outgoing gas;
- Control block.
Specifications
General installation information
Installation weight, no more than kg |
100 |
Overall dimensions of the installation, no more than mm |
800×530×1800 |
Installed power supply, kW |
4,0 |
Maximum working pressure, MPa |
10,0 |
Maximum operating temperature, °С |
900 |
Communication with a computer (sensor monoblock) via Ethernet interfaces |
USB, RS232 |
Gas-phase blast preparation unit
Number of lines, pcs. |
2 (more - by agreement) |
Work with aggressive gases |
by agreement |
Flow regulator |
mass flow controller Bronkhorst High-Tech |
Minimum flow, nl/h |
0,1 |
Maximum flow, nl/h |
50 |
Accuracy (from full scale), % |
± 0,5 |
Accuracy (from indications), % |
± 0,1 |
Block for the preparation of carbonaceous raw materials
Vortex electromagnetic homogenizer |
|
Supply voltage, V |
380 |
Consumed current, A |
7,2 |
Reactor working zone heating temperature, °C |
120-600 |
Working area diameter, mm |
70 |
Reactor volume, L |
0,5-0,75 |
Magnetic field strength in the near-wall zone, not less than Tc |
0,1 |
Product surface temperature, °С |
55 |
Mass of processed material, kg |
0,5 |
Feeding unit for carbonaceous raw materials
Piston metering pump |
|
Working pressure, MPa |
0,1-10,0 |
Working temperature, °С |
25-200 (> 200 °С по согласованию) |
Flow rate, g/h |
10-1000 |
Reactor block
Reactor volume, cm3 |
10 |
Working pressure, MPa |
0,1-10,0 |
Working temperature, °С |
1100 (> 1100 °С by agreement) |
Reactor material |
stainless steel 316 SS |
Reactor diameter, mm |
16 |
Number of thermocouple pockets, pcs |
1 (more - by agreement) |
Heater |
Electric, ceramic |
Movement of raw materials |
In-line |
Pressure control |
Manometer, pressure sensor |
Separation, cleaning and drying unit
Separator |
Centrifugal |
Cooling |
Water, air |
Volume, cm3 |
200 (more - as agreed) |
Working pressure, MPa |
0,1-10,0 |
Working temperature, °С |
25-200 |
Material |
stainless steel 316 SS, 08X18H10T |
Scrubber |
|
Absorbent |
water |
Volume, cm3 |
200 (more - as agreed) |
Working pressure, MPa |
0,1-10,0 |
Working temperature, °С |
25-50 |
Material |
stainless steel 316 SS, 08X18H10T |
Absorbent |
zeolites, silica gel, aluminum oxide |
Volume, cm3 |
50 (more - as agreed) |
Working pressure, MPa |
0,1-10,0 |
Рабочая температура, °С |
25-100 |
Material |
stainless steel 316 SS, 08X18H10T |
Sampling unit
Manual sampling |
|
Automatic sampling |
by agreement |
Unit for measuring the volume of outgoing gas
Gas meter WS-1 |
Precision gas meter WS-1 with liquid seal |
Maximum flow, dm3/h |
1 |
Minimum consumption, dm3/h |
600 |
Limits of permissible relative error, % |
|
Ambient temperature range, °C |
|
Operating environment temperature range, °C |
|
Overall dimensions (W×H×D), mm |
253×260×204 |
Weight, kg |
2,9 (with water 5.5) |
Control block
Monitoring and control of process parameters |
Software, SCADA scheme |
Displaying parameters online |
SCADA diagram |
Recording Process Parameters |
Data archiving |